New Elaborated Technique for Isolation and Purification of Limonene from Orange Oil
نویسندگان
چکیده مقاله:
Essential oil of the orange peel which was extracted by hydrodistillation method showed 50 different mono- and sesquiterpenes on GC-MS analysis, in which limonene had the highest percentage (92.4%). Due to various important uses of the compound, a method was developed for isolation and purification of limonene. In this method, for extra purification, a fractional distillation on Vigreux column under 100 mm Hg vacuum was used which resulted in 96.7% purity for limonene. Subsequent chromatography by two different packages of silica gel and active charcoal columns resulted in 99.4% and 99.9 % purity of limonene, respectively.
منابع مشابه
new elaborated technique for isolation and purification of limonene from orange oil
essential oil of the orange peel which was extracted by hydrodistillation method showed 50 different mono- and sesquiterpenes on gc-ms analysis, in which limonene had the highest percentage (92.4%). due to various important uses of the compound, a method was developed for isolation and purification of limonene. in this method, for extra purification, a fractional distillation on vigreux column ...
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عنوان ژورنال
دوره 2 شماره 2
صفحات 87- 90
تاریخ انتشار 2006-04-01
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